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1、東北師范大學(xué)碩士學(xué)位論文Incpationofferrocenesulfoniccarboxylicacidintopolyanilinefilm:Synthesisapplications姓名：NDAMANISHAJeanChrysostome申請(qǐng)學(xué)位級(jí)別：碩士專業(yè)：AnalyticalChemistry指導(dǎo)教師：LipingGuo20050601AbstractPolyanilinehasattractedgreatInterest
2、inrecentyearsduetohisenvironmentalstabilityandeaseofsynthesisItisnOWknownthatthepropertiesofpolyanilinecanbeimprovedbychangingexperimentalconditionsOurworkthatfocusesattentiononpolyanilineincorporatedwithferroccnesullbni
3、ccarboxylicacidhasmainlythreepartsInthefirstpart，electrochemicalpolymerizationofanilineinthepresenceofferrrocenesulfonicarboxylicacid(S03HFcCOOH)isstudiedandtheresultsshowthatSO’HFcCOOHprotonatespolyanilineduringelectrod
4、eposjtionofthefilmAlsotheincorporationofS03HFcCOOHisconfirmedbyIR，UVVisiblespectraandtheoreticalstudies，TheactionofammoniaonthepolymershowstheinfluenceoftheincorporatedsubstanceThesecondpartcorrespondstotheapplicationoft
5、hepolyanilinefilmsynthesized(PANl一Vc)intheelectrocata[yticoxidationot、methanol(CH30H)’fhisreactionisimportantinviewofitsapplicationinfuel—cellsItisfoundthatCH30HadsorbsonPANI—Fcelectrodebeforeitselectrocatalyticoxidation
6、andthemethanoloxidationCallstartat2MCH30HAtlast，anotherapplicationofthefilm，theelectrocatalyticoxidationoftheophylline，isstudiedwithcyclicvoltammetry(CV)anddifferentialpulsevoltammetl3(DPV)Itsuseasatherapeuticagentnecess
7、itatesclosestudybecausethemetabolismoftheophyllinevariesbetweenjndividualsPANI—Fcelectrodeexhibitsallerdaancementol、thecurrentresponsecomparedtoabareglassycarbonelectrodeinpH6phosphatesolutionThecalibrationcurveislinearw
8、ithadetectionlimitof1339MwhenCVisusedwhereasitis514pMinthecaseofDPVTheresultsshowthatthedeterminationoftheophyllianingreenteaispossibleandtheDPViSmoresensitivethanCVKeywords：Polyaniline，ferrocesullbnicarbonicacid；incorpo
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